From The Swiss Federal Institute of Technology in Lausanne [EPFL-École Polytechnique Fédérale de Lausanne] (CH): “3D images reveal link between crack complexity and material toughness”

From The Swiss Federal Institute of Technology in Lausanne [EPFL-École Polytechnique Fédérale de Lausanne] (CH)

3.28.24
Celia Luterbacher

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Rendering of 3D crack front data. EPFL/EMSI CC BY SA 4.0

By capturing a rare glimpse into three-dimensional crack formation in brittle solids, EPFL researchers have found that complex cracks require more energy to advance than simple ones; a discovery that could improve materials testing and development.

The last time you dropped a favorite mug or sat on your glasses, you may have been too preoccupied to take much notice of the intricate pattern of cracks that appeared in the broken object. But capturing the formation of such patterns is the specialty of John Kolinski and his team at the Laboratory of Engineering Mechanics of Soft Interfaces (EMSI) in EPFL’s School of Engineering. They aim to understand how cracks propagate in brittle solids, which is essential for developing and testing safe and cost-effective composite materials for use in construction, sports, and aerospace engineering.

But traditional mechanics approaches to analyzing crack formation assume that cracks are planar – i.e., that they form on the two-dimensional surface of a material. In fact, simple planar cracks are just the tip of the iceberg: most cracks – like those in everyday brittle solids like glass – propagate into three-dimensional networks of ridges and other complex features.

Due to material opacity and the speed with which cracks form, observing this complexity in real time is extremely difficult. But now, armed with a Swiss Army knife and a confocal microscope, Kolinski and his team have managed to do just that – and they have discovered a positive correlation between crack complexity and material toughness in the process.

“The energy required to drive cracks has traditionally been considered a material property, but our work yields unique insights into the key role of geometry: namely, that by increasing the complexity of geometric features at the crack tip, a material can be made effectively tougher, because more strain energy is required to advance a complex crack than a simple one,” Kolinski says. “This highlights an important gap in the current theory for 3D cracks.”

The lab’s results have recently been published in Nature Physics.
See the science paper for instructive material with images.

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The scientists induced cracks with a standard Swiss Army knife. EPFL/EMSI CC BY SA 4.0

A fundamental link between length and strength

The researchers’ method involved creating very thin slices of four different hydrogels and an elastomer. Transparent and brittle, but easy to deform and measure without shattering, the hydrogels served as a proxy for understanding how cracks form in glass and brittle plastics. The elastomer was likewise a proxy for materials like rubber and silicone polymers.

While the experimental cracks were observed with a state-of-the-art confocal microscope, they were induced using a standard Swiss Army knife: the shearing action of the device’s scissors naturally produced geometrically complex cracks in the hydrogel samples. Using a custom apparatus developed by the EMSI team to control sample alignment and loading, a series of fluorescent images was generated with the confocal microscope, and then stacked to assemble a unique, three-dimensional map of each fracture surface.

“People have long known that cracks can become complex by looking at fracture surfaces after the fact, but what is lost is the understanding of the loading conditions when the crack emerged, or what forces the sample was exposed to,” Kolinski explains. “Our innovative imaging method has made it possible to characterize this relationship rigorously in-situ.”

In a nutshell, these experiments revealed that the strain energy required to drive the sample cracks was directly proportional to the lengths of the crack tips. This suggests that the increased geometric complexity of a 3D crack generates more fracture surface as the crack advances, thus requiring additional strain energy to drive it.

In another experiment, the researchers showed how, as a smoother crack approached a rigid obstacle embedded in the sample, the crack’s planar symmetry was broken, increasing both the crack tip length and the energy required to drive the crack forward.

“The fact that we can isolate how geometric complexity emerges with such an inhomogeneity in the material could motivate new design approaches,” Kolinski says. “Our work also highlights the importance of care in carrying out materials testing, as we now know that any geometric deviation from a planar crack front may lead to a mis-measurement – and potentially dangerous over-estimation – of material toughness.”

See the full article here .

Comments are invited and will be appreciated, especially if the reader finds any errors which I can correct.

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The Swiss Federal Institute of Technology in Lausanne [EPFL-École Polytechnique Fédérale de Lausanne] (CH) is a research institute and university in Lausanne, Switzerland, that specializes in natural sciences and engineering. It is one of the two Swiss Federal Institutes of Technology, and it has three main missions: education, research and technology transfer.

The QS World University Rankings ranks EPFL(CH) very high, whereas Times Higher Education World University Rankings ranks EPFL(CH) as one of the world’s best schools for Engineering and Technology.

EPFL(CH) is located in the French-speaking part of Switzerland; the sister institution in the German-speaking part of Switzerland is The Swiss Federal Institute of Technology ETH Zürich [Eidgenössische Technische Hochschule Zürich] (CH). Associated with several specialized research institutes, the two universities form The Domain of the Swiss Federal Institutes of Technology (ETH Domain) [ETH-Bereich; Domaine des Écoles Polytechniques Fédérales] (CH) which is directly dependent on the Federal Department of Economic Affairs, Education and Research. In connection with research and teaching activities, EPFL(CH) operates a nuclear reactor CROCUS; a Tokamak Fusion reactor; a Blue Gene/Q Supercomputer; and P3 bio-hazard facilities.

ETH Zürich, EPFL (Swiss Federal Institute of Technology in Lausanne) [École Polytechnique Fédérale de Lausanne](CH), and four associated research institutes form The Domain of the Swiss Federal Institutes of Technology (ETH Domain) [ETH-Bereich; Domaine des Écoles polytechniques fédérales] (CH) with the aim of collaborating on scientific projects.

The roots of modern-day EPFL(CH) can be traced back to the foundation of a private school under the name École Spéciale de Lausanne in 1853 at the initiative of Lois Rivier, a graduate of the École Centrale Paris (FR) and John Gay the then professor and rector of the Académie de Lausanne. At its inception it had only 11 students and the offices were located at Rue du Valentin in Lausanne. In 1869, it became the technical department of the public Académie de Lausanne. When the Académie was reorganized and acquired the status of a university in 1890, the technical faculty changed its name to École d’Ingénieurs de l’Université de Lausanne. In 1946, it was renamed the École polytechnique de l’Université de Lausanne (EPUL). In 1969, the EPUL was separated from the rest of the University of Lausanne and became a federal institute under its current name. EPFL(CH), like ETH Zürich (CH), and it is thus directly controlled by the Swiss federal government. In contrast, all other universities in Switzerland are controlled by their respective cantonal governments. EPFL(CH) has started to develop into the field of life sciences. It absorbed the Swiss Institute for Experimental Cancer Research (ISREC) in 2008.

In 1946, there were 360 students. In 1969, EPFL(CH) had 1,400 students and 55 professors. In the past two decades the university has grown rapidly and over 14,000 people study or work on campus, about 10,000 of these being Bachelor, Master or PhD students. The environment at modern day EPFL(CH) is highly international with the school attracting students and researchers from all over the world. More than 125 countries are represented on the campus and the university has two official languages, French and English.

Organization

EPFL is organized into eight schools, themselves formed of institutes that group research units (laboratories or chairs) around common themes:

School of Basic Sciences
Institute of Mathematics
Institute of Chemical Sciences and Engineering
Institute of Physics
European Centre of Atomic and Molecular Computations
Bernoulli Center
Biomedical Imaging Research Center
Interdisciplinary Center for Electron Microscopy
MPG-EPFL Centre for Molecular Nanosciences and Technology
Swiss Plasma Center
Laboratory of Astrophysics

School of Engineering

Institute of Electrical Engineering
Institute of Mechanical Engineering
Institute of Materials
Institute of Microengineering
Institute of Bioengineering

School of Architecture, Civil and Environmental Engineering

Institute of Architecture
Civil Engineering Institute
Institute of Urban and Regional Sciences
Environmental Engineering Institute

School of Computer and Communication Sciences

Algorithms & Theoretical Computer Science
Artificial Intelligence & Machine Learning
Computational Biology
Computer Architecture & Integrated Systems
Data Management & Information Retrieval
Graphics & Vision
Human-Computer Interaction
Information & Communication Theory
Networking
Programming Languages & Formal Methods
Security & Cryptography
Signal & Image Processing
Systems

School of Life Sciences

Bachelor-Master Teaching Section in Life Sciences and Technologies
Brain Mind Institute
Institute of Bioengineering
Swiss Institute for Experimental Cancer Research
Global Health Institute
Ten Technology Platforms & Core Facilities (PTECH)
Center for Phenogenomics
NCCR Synaptic Bases of Mental Diseases

College of Management of Technology

Swiss Finance Institute at EPFL
Section of Management of Technology and Entrepreneurship
Institute of Technology and Public Policy
Institute of Management of Technology and Entrepreneurship
Section of Financial Engineering

College of Humanities

Human and social sciences teaching program

EPFL Middle East

Section of Energy Management and Sustainability

In addition to the eight schools there are seven closely related institutions

Swiss Cancer Centre
Center for Biomedical Imaging (CIBM)
Centre for Advanced Modelling Science (CADMOS)
École Cantonale d’art de Lausanne (ECAL)
Campus Biotech
Wyss Center for Bio- and Neuro-engineering
Swiss National Supercomputing Centre

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