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  • richardmitnick 3:27 pm on September 15, 2014 Permalink | Reply
    Tags: , , DESY, PETRA III, ,   

    From DESY: “Double topping-out celebrations at DESY” 

    DESY
    DESY

    Two new experimental halls for research light source PETRA III

    Today DESY celebrates the topping-out of two large experimental halls for the research light source PETRA III.Ten additional beamlines, which will serve in the PETRA III particle accelerator’s high intensity X-ray experiments, are under construction in a space measuring approximately 6000 square meters; the facility will also include en-suite offices and laboratory spaces for scientists.The experimentation capabilities at the PETRA III synchrotron radiation source will be considerably increased due to the expansion project.The first new beamlines of the 80-million-Euro-project will be ready for operation beginning in autumn 2015.
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    pit

    “With the new experimental stations, we are significantly expanding the research capabilities of PETRA III, for example, with new nanospectroscopy and materials research technologies,” says Chairman of the DESY Board of Directors Professor Helmut Dosch at the event. “At the same time, we will be fulfilling the enormous worldwide scientific demand for the best synchrotron radiation source in the world.”

    Hamburg´s Science Senator Dr. Dorothee Stapelfeldt says: “The senate’s aim is to develop Hamburg into one of the leading locations for research and innovation in Europe.In order to do so, it is essential to further raise the profiles of universities and research institutions in close dialogue with all stakeholders.Hamburg already occupies a leading position in structural research.The ground-breaking cooperation between DESY, the university and their partners at the Bahrenfeld research campus has been clearly recognized internationally.With the two new experimental halls, PETRA’s synchrotron radiation will be made available to even more researchers from all over the world in the future.”

    “With a total of ten new beamlines, the allure of Hamburg as a location for cutting-edge research will continue to increase, nationally and internationally,” says Dr. Beatrix Vierkorn-Rudolph (BMBF), Chairperson of the DESY Foundation Council. “With its excellent research opportunities, PETRA III contributes to rapidly transfering the results of basic research into application while also strengthening the innovative power of Germany.”

    DESY’s 2.3-kilometre-long PETRA III ring accelerator produces high intensity, highly collimated X-ray pulses for a diverse range of physical, biological and chemical experiments.Fourteen measuring stations, which can accommodate up to thirty experiments, already exist in an approximately 300-metre-long experimental hall.The properties of light pulses, which PETRA delivers to the different measuring stations, are thereby precisely attuned to the different research disciplines.Using the extremely brilliant X-rays, researchers study, for example, innovative solar cells, observe the dynamics of cell membranes and analyse fossilised dinosaur eggs.

    PETRA III, the world´s best X-ray source of its kind, has been heavily over-booked since it began operations in 2009.The PETRA III Extension Project was begun in December 2013 to give more scientists access to the unique experimental possibilities of this research light source and to broaden PETRA III’s research portfolio in experimental technologies:measuring approximately 6000 square meters in their entirety, the two new experimental halls house enough space for technical installations of up to ten additional beam lines, and an additional 1400 square metres provide office and laboratory space for the scientists.The beam lines and measuring instruments in the new halls are under construction in close cooperation with the future user community and are, in part, collaborative research projects.Three of the future PETRA beamlines will be constructed as an international partnership with Sweden, India and Russia.

    Altogether approximately 170 metres of the PETRA tunnel and accelerator have been dismantled since February to build the new experimental halls. Since August, the accelerator, equipped with special magnets for producing X-ray radiation, has been under reconstruction within the new tunnel areas that have already been completed.After the preliminary construction phase of the experimental halls, they are to be developed further from December 2014 onward; the accelerator will at the same time resume operation.The experiments will re-start in the PETRA III experimental hall “Max von Laue” beginning in April 2015 and the first measuring stations in the new, still unnamed halls should gradually become ready for operation in autumn 2015 and the start of 2016.

    The extension’s total budget of approximately 80 million Euros stems in large part from the Helmholtz Association’s expansion funds as well as funds from the Federal Ministry of Research, the Free and Hanseatic City of Hamburg and DESY.Collaborative partners from Germany and abroad cover approximately one third of the costs.

    See the full article here.

    desi

    DESY is one of the world’s leading accelerator centres. Researchers use the large-scale facilities at DESY to explore the microcosm in all its variety – from the interactions of tiny elementary particles and the behaviour of new types of nanomaterials to biomolecular processes that are essential to life. The accelerators and detectors that DESY develops and builds are unique research tools. The facilities generate the world’s most intense X-ray light, accelerate particles to record energies and open completely new windows onto the universe. 
That makes DESY not only a magnet for more than 3000 guest researchers from over 40 countries every year, but also a coveted partner for national and international cooperations. Committed young researchers find an exciting interdisciplinary setting at DESY. The research centre offers specialized training for a large number of professions. DESY cooperates with industry and business to promote new technologies that will benefit society and encourage innovations. This also benefits the metropolitan regions of the two DESY locations, Hamburg and Zeuthen near Berlin.

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  • richardmitnick 3:43 pm on September 12, 2014 Permalink | Reply
    Tags: , , DESY, ,   

    From DESY: “Researchers X-Ray Living Cancer Cells” 

    DESY
    DESY

    27.02.2014

    Nanodiffraction opens up new insights into the physics of life

    Göttingen-based scientists working at DESY’s PETRA III research light source have carried out the first studies of living biological cells using high-energy X-rays. The new method shows clear differences in the internal cellular structure between living and dead, chemically fixed cells that are often analysed. “The new method for the first time enables us to investigate the internal structures of living cells in their natural environment using hard X-rays,” emphasises the leader of the working group, Prof. Sarah Köster from the Institute for X-Ray Physics of the University of Göttingen. The researchers present their work in the scientific journal Physical Review Letters.
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    c ells
    X-ray scan of chemically fixed cells. Each pixel represents a full diffraction image. The colours indicate how strong the X-rays are scattered at each individual point. Credit: Britta Weinhausen/University of Göttingen

    Thanks to analytical methods with ever-higher resolution, scientists today can study biological cells at the level of individual molecules. The cells are frequently chemically fixed before they are studied with the help of optical, X-ray or electron microscopes. The process of chemical fixation involves immersing the cells in a type of chemical preservative which fixes all of the cell’s organelles and even the proteins in place. “Minor changes to the internal structure of the cells are unavoidable in this process,” emphasises Köster. “In our studies, we were able to show these changes in direct comparison for the first time.”

    The team used cancer cells from the adrenal cortex for their analyses. They grew the cells on a silicon nitrite substrate, which is almost transparent to X-rays. In order to keep the cells alive in the experimental chamber during the experiment, they were supplied with nutrients, and their metabolic products were pumped away via fine channels just 0.5 millimetres in diameter. “The biological cells are thus located in a sample environment which very closely resembles their natural environment,” explains Dr. Britta Weinhausen from Köster’s group, the paper’s first author.

    The experiments were carried out at the Nanofocus Setup (GINIX) of PETRA III’s experimental station P10. The scientists used the brilliant X-ray beam from PETRA III to scan the cells in order to obtain information about their internal nanostructure. “Each frame was exposed for just 0.05 seconds, in order to avoid damaging the living cells too quickly”, explains co-author Dr. Michael Sprung from DESY. “Even nanometre-scale structures can be measured with the GINIX assembly, thanks to the combination of PETRA III’s high brilliance and the GINIX setup which is matched to the source.”

    The researchers studied living and chemically fixed cells using this so-called nanodiffraction technique and compared the cells’ internal structures on the basis of the X-ray diffraction images. The results showed that the chemical fixation produces noticeable differences in the cellular structure on a scale of 30 to 50 nanometres (millionths of a millimetre).

    “Thanks to the ever-greater resolution of the various investigative techniques, it is increasingly important to know whether the internal structure of the sample changes during sample preparation,” explains Köster. In future, the new technique will make it possible to study unchanged living cells at high resolution. Although other methods have an even higher resolution than X-ray scattering, they require a chemical fixation or complex and invasive preparation of the cells. Lower-energy, so-called soft X-rays have already been used for studies of living cells. However, the study of structures with sizes as small as 12 nanometres first becomes possible through the analysis of diffraction images produced using hard X-rays.

    See the full article here.

    desi

    DESY is one of the world’s leading accelerator centres. Researchers use the large-scale facilities at DESY to explore the microcosm in all its variety – from the interactions of tiny elementary particles and the behaviour of new types of nanomaterials to biomolecular processes that are essential to life. The accelerators and detectors that DESY develops and builds are unique research tools. The facilities generate the world’s most intense X-ray light, accelerate particles to record energies and open completely new windows onto the universe. 
That makes DESY not only a magnet for more than 3000 guest researchers from over 40 countries every year, but also a coveted partner for national and international cooperations. Committed young researchers find an exciting interdisciplinary setting at DESY. The research centre offers specialized training for a large number of professions. DESY cooperates with industry and business to promote new technologies that will benefit society and encourage innovations. This also benefits the metropolitan regions of the two DESY locations, Hamburg and Zeuthen near Berlin.

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  • richardmitnick 3:31 pm on September 12, 2014 Permalink | Reply
    Tags: , DESY,   

    From DESY: “Scientists watch nanoparticles grow” 

    DESY
    DESY

    27.03.2014
    No Writer Credit

    Analysis allows tailoring materials for switchable windows and solar cells

    With DESY’s X-ray light source PETRA III, Danish scientists observed the growth of nanoparticles live. The study shows how tungsten oxide nanoparticles are forming from solution. These particles are used for example for smart windows, which become opaque at the flick of a switch, and they are also used in particular solar cells. The team around lead author Dr. Dipankar Saha from Århus University present their observations in the scientific journal Angewandte Chemie – International Edition.
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    nano
    Top: Structure of the ammonium metatungstate dissolved in water on atomic length scale. The octahedra consisting of the tungsten ion in the centre and the six surrounding oxygen ions partly share corners and edges. Bottom: Structure of the nanoparticles in the ordered crystalline phase. The octahedra exclusively share corners. Credit: Dipankar Saha/Århus University

    For their investigation, the scientists built a small reaction chamber, which is transparent for X-rays. “We use fine capillaries of sapphire or fused silica which are easily penetrable by X-rays,” said Professor Bo Iversen, head of the research group. In these capillaries, the scientists transformed so-called ammonium metatungstate dissolved in water into nanoparticles at high temperature and high pressure. With the brilliant PETRA III X-ray light, the chemists were able to track the growth of small tungsten trioxide particles (WO3) with a typical size of about ten nanometres from the solution in real time.

    “The X-ray measurements show the building blocks of the material,” said co-author Dr. Ann-Christin Dippel from DESY, scientist at beamline P02.1, where the experiments were carried out. “With our method, we are able to observe the structure of the material at atomic length scale. What is special here is the possibility of following the dynamics of the growth process,” Dippel points out. “The different crystal structures that form in these nanoparticles are already known. But now we can track in real-time the transformation mechanism of molecules to nanocrystals. We do not only see the sequence of the process but also why specific structures form.”

    On the molecular level, the basic units of many metal-oxygen compounds like oxides are octahedra, which consist of eight equal triangles. These octahedra may share corners or edges. Depending on their configuration, the resulting compounds have different characteristics. This is not only true for tungsten trioxide but is basically applicable to other materials.

    The octahedra units in the solutions grow up to nanoparticles, with a ten nanometre small particle including about 25 octahedra. “We were able to determine that at first, both structure elements exist in the original material, the connection by corners and by edges,” said Saha. “In the course of the reaction, the octahedra rearrange: the longer you wait, the more the edge connection disappears and the connection by corners becomes more frequent. The nanoparticles which developed in our investigations have a predominantly ordered crystal structure.”

    In the continuous industrial synthesis, this process occurs so quickly, that it mainly produces nanoparticles with mixed disordered structures. “Ordered structures are produced when nanoparticles get enough time to rearrange,” said Saha. “We can use these observations for example to make available nanoparticles with special features. This method is also applicable to other nanoparticles.”

    See the full article here.

    desi

    DESY is one of the world’s leading accelerator centres. Researchers use the large-scale facilities at DESY to explore the microcosm in all its variety – from the interactions of tiny elementary particles and the behaviour of new types of nanomaterials to biomolecular processes that are essential to life. The accelerators and detectors that DESY develops and builds are unique research tools. The facilities generate the world’s most intense X-ray light, accelerate particles to record energies and open completely new windows onto the universe. 
That makes DESY not only a magnet for more than 3000 guest researchers from over 40 countries every year, but also a coveted partner for national and international cooperations. Committed young researchers find an exciting interdisciplinary setting at DESY. The research centre offers specialized training for a large number of professions. DESY cooperates with industry and business to promote new technologies that will benefit society and encourage innovations. This also benefits the metropolitan regions of the two DESY locations, Hamburg and Zeuthen near Berlin.

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  • richardmitnick 1:20 pm on January 4, 2012 Permalink | Reply
    Tags: , DESY, , , ,   

    From SLAC News Center: “LCLS Teams Up with DESY on Shortest X-ray Exposure of a Protein Crystal Ever” 

    January 4, 2012
    from Deutsches Elektronen-Synchrotron DESY

    “An international research team headed by DESY scientists from the Center for Free-Electron Laser Science (CFEL) in Hamburg, Germany, has recorded the shortest X-ray exposure of a protein crystal ever achieved. The incredible brief exposure time of 30 femtoseconds (0.000 000 000 000 03 seconds) opens up new possibilities for imaging molecular processes with X-rays.

    This is of particular interest to biologists, but can be employed in many fields, explain lead authors Dr. Anton Barty and Prof. Henry Chapman from the German accelerator centre Deutsches Elektronen-Synchrotron DESY. CFEL is a joint venture of DESY, the Max Planck Society and the University of Hamburg.

    From X-ray diffraction the molecular structure of proteins can be determined. The shorter the X-ray pulse and the higher its intensity, the better the structural information gained. With the free-electron laser at the SLAC National Accelerator Laboratory’s Linac Coherent Light Source (LCLS), the research team fired the most intense X-ray beam at a protein crystal to date: The tiny crystal was bombarded with a whamming 100,000 trillion watts per square centimeter – sunlight for comparison comes in at a mere 0.1 watts per square centimeter on average.

    ‘This way we get the most information out of the smallest crystals’, Chapman explains. Having small crystals is important, as especially many biological substances aren’t easily crystallized.

    cr
    The molecular structure of proteins is inferred by measurements of patterns of X-rays scattered from crystals formed from those proteins. The regular array of molecules in the crystal gives rise to strong peaks needed for measurement, shown here as balls in a three-dimensional space.

    Image courtesy Thomas White, CEFL/DESY

    Full announcement posted Dec. 19, 2011, on DESY website.”

    SLAC is a multi-program laboratory exploring frontier questions in photon science, astrophysics, particle physics and accelerator research. Located in Menlo Park, California, SLAC is operated by Stanford University for the DOE’s Office of Science. i1

     
  • richardmitnick 5:13 pm on December 9, 2011 Permalink | Reply
    Tags: , , DESY, , , ,   

    From ilc newsline: “LCIO 2.0 improves simulation coordination’ 

    Leah Hesla
    8 December 2011

    “The data model that transformed the linear collider detector community from a computational Tower of Babel into a group that inputs with one voice has gotten an update.

    ILC software developers released LCIO. 2.0 this autumn. The new version of LCIO, a particle event data model, includes features that help scientists cope with the increasingly sophisticated data being fed into particle event simulations.

    ‘We considerably improved the data model – in particular for the description of charged particle tracks – and put in little things from users’ requests or features we thought would improve physicists’ lives,’ said DESY’s Frank Gaede, one of the main developers of LCIO and coordinator of ILCSoft, one of two software packages for which LCIO is the core.”

    i3
    Illustration of the way LCIO works with multiple software formats. Image: DESY

    i5
    A t t event simulated and reconstructed using ILCSoft, one of two software programs with LCIO at its core. Image: DESY

    See the full article here.

     
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