From Brookhaven Lab: “New Technique Uses Electrons to Map Nanoparticle Atomic Structures”

Brookhaven Lab

Accessibility of electron microscopes could make technique standard practice

May 4, 2012
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“With dimensions measuring billionths of a meter, nanoparticles are way too small to see with the naked eye. Yet it is becoming possible for today’s scientists not only to see them, but also to look inside at how the atoms are arranged in three dimensions using a technique called nanocrystallography. Trouble is, the powerful machines that make this possible, such as x-ray synchrotrons, are only available at a handful of facilities around the world. The U.S. Department of Energy’s Brookhaven National Laboratory is one of them — home to the National Synchrotron Light Source (NSLS) and future NSLS-II, where scientists are using very bright, intense x-ray beams to explore the small-scale structure of new materials for energy applications, medicine, and more.

But a Brookhaven/Columbia Engineering School team of scientists, in collaboration with researchers at DOE’s Argonne National Laboratory (ANL) and Northwestern University, has also been working to develop nanocrystallography techniques that can be used in more ordinary science settings. They have shown how a powerful method called atomic pair distribution function (PDF) analysis — which normally requires synchrotron x-rays or neutrons to discern the atomic arrangements in nanoparticles — can be carried out using a transmission electron microscope (TEM) — an instrument found in many chemistry and materials science laboratories.”

This could be very exciting. See the full article here.

National Synchrotron Light Source (NSLS)


One of ten national laboratories overseen and primarily funded by the Office of Science of the U.S. Department of Energy (DOE), Brookhaven National Laboratory conducts research in the physical, biomedical, and environmental sciences, as well as in energy technologies and national security. Brookhaven Lab also builds and operates major scientific facilities available to university, industry and government researchers. Brookhaven is operated and managed for DOE’s Office of Science by Brookhaven Science Associates, a limited-liability company founded by Stony Brook University, the largest academic user of Laboratory facilities, and Battelle, a nonprofit, applied science and technology organization.

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